Patrón de difracción Debye-Scherrer de muestras de polvoscon estructura de diamante (geometría Bragg-Brentano)

Num.Producto: P2542201
Principle

Polycrystalline powder samples, which crystallize in the three cubic Bravais types, simple, face-centered and body-centered, are irradiated with the radiation from a Roentgen tube with a copper anode. A swivelling Geiger-Mueller counter tube detects the radiation that is constructively reflected from the various lattice planes of the crystallites. The Bragg diagrams are automatically recorded. Their evaluation gives the assignment of the Bragg lines to the individual lattice planes, their spacings as well as the lattice constants of the samples, and so also the corresponding Bravais lattice type.

Tasks

  1. Record the intensity of the Cu X-rays back scattered by the four cubic crystal powder samples with various Bravais lattice types as a function of the scattering angle.
  2. Calculate the lattice plane spacings appropriate to the angular positions of the individual Bragg lines.
  3. Assign the Bragg reflections to the respective lattice planes. Determine the lattice constants of the samples and their Bravais lattice types.
  4. Determine the number of atoms in the unit cell.

What you can learn about

  • Crystal lattices
  • Crystal systems
  • Bravais-lattice
  • Reciprocal lattice
  • Miller indices
  • Structure factor
  • Atomic scattering factor
  • Bragg scattering
  • Characteristic X-rays
  • Monochromatization of X-rays
  • Bragg Brentano geometry

Lista de material (extracto) Producto Cantidad
XR 4.0 Unidad de rayos X, 35 kV 09057-99 1
X-ray MODULO ENCHUFABLE CON TUBO DE RAYOS X DE COBRE 09057-51 1
XR 4.0 X-ray goniometro 09057-10 1
XR 4.0 Software measure X-ray 14414-61 1
POLVO DE GERMANIO, 99%, 10 g 31768-03 1
Tubo contador Geiger-Mueller tipo B 09005-00 1
CRISTAL FLUORO DE LITIO 09056-05 1
X-ray SOPORTE UNIVERSALO DE CRISTALES PARA UNIDAD DE RAYOS X 09058-02 1
TUBO D.DIAFRAGMA C.LAMINA D.NI 09056-03 1
XR 4.0 X-ray TUBO D.DIAFRAGMA d = 2 mm 09057-02 1
Silicio en polvo fino, 50 g 31155-05 1
X-ray SUPPORTE PARA MUESTRAS DE POLVO (DIFRACTOMETRIA) 09058-09 1
Cable de datos USB, hembra tipo A/B, 1,8 m 14608-00 1
Mortero de porcelana, d=80 mm 32603-00 1
VASELINA, 100G 30238-10 1
Microespátula de acero inoxidable, l=150 milímetros 33393-00 1

A continuación la literatura para este producto

Título Producto Idioma
Handbuch Lehrerversuche mit Röntgenstrahlung für die XR 4.0 expert unit, TESS expert Physik 01200-01 DEU
TESS expert Physics Handbook X-ray Experiments for XR 4.0 expert unit 01200-02 ENG
XRS 4.0 X-ray Strukturanalyse Erweiterungsset 09140-88

regresar a la lista correspondiente

Product No: P2542201

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